There is plenty of material available on the net, I found this here pretty useful:
Diplexer from Tonne Software (a very efficient specialized design tool which allows to play with the values and see the effect)
RFSIM (a general purpose RF simulation tool. Not ideal for a diplexer as it only allows simulation of two ports but still good to see a single filter)
DF6VB's instructions for building a diplexer (which are very close to how mine works - only in German though)
